Question- which of the following would techniques would be, Chemistry

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Question- which of the following would techniques would be

Question- Which of the following would techniques would be most appropriate to show that the diazonium reaction was successful?
1H â€"NMR b. 13C-NMR c. IR d. MS

1) Why is it a bad idea to isolate a diazonium salt?

Please illustrate work if possible thanks

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