At 60oc 2000 kg of aqueous reaction mixture can be cooled
At 60oC 2000 kg of aqueous reaction mixture can be cooled at a rate of 0.5oC/min.
What cooling power does this correspond to?
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Semi-batch isothermal calorimetry in SIMULAR at 60oC involving a single phase organic reaction mixture show that with a dosing period of one hour the reaction is feed rate limited with no accumulation.
If this process was carried out as an all in batch reaction estimate the maximum temperature if cooling were lost just as the reactants were mixed?
Thermal stability studies indicate a gas generating, exothermic decomposition from 150oC. If the reaction mixture boils at 185 oC then what is the criticality class of the all in batch process?
At 60oC 2000 kg of aqueous reaction mixture can be cooled at a rate of 0.5oC/min. What cooling power does this correspond to?
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How much cooling will be required on the industrial recipe scale of 1000 kg? Allow a safety margin of 20%.
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